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- W3036836070 abstract "Our understanding the nature of interfaces in polycrystalline materials has depended critically on observations obtained in the transmission electron microscope. This is especially true in the case of interfacial structure, where developments in models of atomic and defect structures in interfaces have closely paralleled advances in techniques available for their study. The general acceptance that the crystallography and relative misorientation of the two crystals forming an interface dictate the interfacial structure, and many of its properties, results in large part from direct TEM studies of interfaces. Grain boundaries were originally considered structureless, amorphous, films, because optical microscopy could not provide information at the necessary resolution, and inferences about the nature of boundaries had to be made from measurements of mechanical properties. However, the development of X-ray methods in the 1920's quickly showed that the crystalline structure of the grains was preserved right up to an interface, and that the boundary could be thought of as a “transition lattice” from one crystal to the other, a concept remarkably similar to many of those still current today. Although there was some earlier optical microscopy of decorated low-angle boundaries in Si, it was not until 1956 that the development of the TEM provided the first detailed picture of dislocations and grain boundaries in opaque materials." @default.
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- W3036836070 date "1990-08-01" @default.
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- W3036836070 title "The role of Electron Microscopy in the study of grain boundaries" @default.
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- W3036836070 doi "https://doi.org/10.1017/s0424820100174783" @default.
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