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- W3036837566 abstract "Two inherent problems associated with chromatographic separations are peak broadening and column efficiency. These are directly attributable to the interparticular porosity of the separation media in which limited utilization of column space results in column void volumes. In theory, a minimum of 26% void volume will occur if a column is packed using perfectly arranged monodispersed beads. Typically, with the best packed columns void volumes are 30 to 40%. Svec and Fréchet have introduced an HPLC separation media with no discontinuity that are prepared in a single step by a free-radical polymerization within a column acting as a mold. The resulting rods consist of a continuous molded monolith of rigid, highly porous polymer. These columns proved to be very efficient and extremely fast for reverse-phase HPLC separation of proteins and for the separation of small and mid-size molecules. In this study, we continue to explore various reaction conditions with the resulting polymerization products examined by SEM, for internal morphology." @default.
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- W3036837566 date "1996-08-11" @default.
- W3036837566 modified "2023-09-23" @default.
- W3036837566 title "SEM analysis of in situ polymerization products for chromatographic separations" @default.
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- W3036837566 doi "https://doi.org/10.1017/s0424820100163344" @default.
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