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- W3036908093 abstract "Studies of metal/support interactions in catalytic materials have been facilitated by use of model catalysts consisting of metals deposited on substrates of simple geometry suitable for direct imaging in the transmission electron microscope. An example of such a catalyst/substrate system is a model combustion catalyst comprised of nanometer-sized particles of Pd deposited on amorphous silica microspheres. These materials have recently been characterized both by high resolution TEM imaging and electron holography techniques, as well as by ultra-high resolution SEM imaging. TEM and holography results indicated that the particles, which range from 5 to 15 nm in diameter, were single crystals. In addition, depending upon preparation conditions, these nanocrystals typically contained a single void that was shown by holography to be empty. Figure 1 shows a TEM image of a typical particle on the SiO 2 sphere, where the void is clearly evident. The high resolution SEM imaging results from these specimens of known geometry are presented in this paper." @default.
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- W3036908093 date "1994-01-01" @default.
- W3036908093 modified "2023-09-27" @default.
- W3036908093 title "High-resolution SEM imaging of model catalytic materials" @default.
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- W3036908093 doi "https://doi.org/10.1017/s0424820100172917" @default.
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