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- W3036954018 abstract "Spatially resolved EELS in a STEM provides unique opportunities to examine how local structural and electronic properties can affect macroscopic properties of a solid. Perhaps nowhere else are these connections as pronounced as at interfaces. For instance, H embrittles and B strengthens the grain boundaries in Ni 3 Al, a prototypical high-temperature intermetallic. EELS measurements of these boundaries have revealed the changes in electronic structure that correlate with the altered mechanical properties of the material. The interfacial states, which rarely extend more than an atomic layer or so from the boundary, can only be observed with great care. Not only is a stable microscope and very efficient detector required, but also a good understanding of how the probe interacts with the specimen. Artifacts due to radiation damage are a real possibility. If the boundary is examined in a strongly diffracting orientation (as is often the case with special boundaries) probe dechanneling can profoundly alter the measured spectra. This can be avoided by tilting the boundary a few mrad away from the zone axis, which limits the spatial resolution to being sub-nanometer, but not atomic." @default.
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- W3036954018 date "1996-08-11" @default.
- W3036954018 modified "2023-09-27" @default.
- W3036954018 title "Beyond fingerprinting: simple but quantitative models of EELS fine structure and the cohesion of interfaces" @default.
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- W3036954018 doi "https://doi.org/10.1017/s0424820100165069" @default.
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