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• W3037355974 startingPage "4408" @default.
• W3037355974 abstract "Synthesis of orthogonally protected 2‐silyl nucleosides were achieved by trans opening of sugar epoxides with nucleobases catalyzed by trimethylsilyltrifluoromethanesulfonate using hexamethyldisilazane both as solvent and silylating agent. Both α and β nucleosides were obtained with complete stereocontrol only by changing the epoxide stereochemistry. The synthesized nucleosides exist in different chair conformations depending upon the nature of protecting groups present in the sugar moiety as determined from coupling constants in the proton NMR. All the synthesized nucleosides were screened for biofilm inhibition activity against four bacterial pathogens and compound 7c was found to be most potent against Salmonella typhimurium with 1.22 µ m biofilm inhibitory activity taking ciprofloxacin as control." @default.
• W3037355974 created "2020-07-02" @default.
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• W3037355974 date "2020-07-17" @default.
• W3037355974 modified "2023-09-27" @default.
• W3037355974 title "Synthesis and Conformational Analysis of 2-<i>O</i>-Silyl Protected Nucleosides from Unprotected Nucleobases and Sugar Epoxides" @default.
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• W3037355974 doi "https://doi.org/10.1002/ejoc.202000650" @default.
• W3037355974 hasPublicationYear "2020" @default.
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