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- W303762375 abstract "Abstract The applications and processing of nanostructured materials at high temperatures require stability of their morphology. However, in such environments (>1000 °C), these structures are prone to significant undesired microstructural changes that result in a loss of functional properties. The thermal stability of titania inverse opal films, prepared from self-assembled templates of monodisperse polystyrene spheres by infiltration utilizing atomic layer deposition and subsequent calcination, was assessed. Resistance to grain growth and a shift in the anatase-to-rutile transformation to higher temperatures was observed, with dramatic stability under vacuum. Vacuum annealed samples retained the anatase phase and exhibited minimal grain growth even after 3 h at 1300 °C. Photonic properties were retained until the transformation onset. The remarkable resistance was attributed to inhibition of surface diffusion and structure-substrate constraints. In addition to being technologically enabling, the results provide further insight into the titania system and its phase transformation mechanism." @default.
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- W303762375 date "2015-10-01" @default.
- W303762375 modified "2023-10-18" @default.
- W303762375 title "Enhanced structural and phase stability of titania inverse opals" @default.
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- W303762375 doi "https://doi.org/10.1016/j.jeurceramsoc.2015.04.041" @default.
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