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- W3037665956 abstract "Reversible-deactivation radical polymerizations (RDRP) of acrylamide (AM) was carried out via dispersion polymerization mediated by cobalt complexes in alcohol/water and initiated by azobisisobutyronitrile (AIBN) at 65 °C. Well-defined polyacrylamide (PAM) uniform spherical particles with predetermined molecular weight and relatively narrow dispersity (Đ = 1.24–1.53) were obtained under mild thermal conditions based on one polymer chain per cobalt complex demonstrate the living characters of the polymerization process. The living character was demonstrated by the linear fit with different feeding ratios of AM and cobalt complex, as well as a linear increase in the number- average molecular weight observed with the monomer conversion. It is worth pointing out that the high conversion of AM (>90%) was obtained with formation of well-controlled PAM, relative to the cobalt porphyrin (The conversion of AM reached 40%) in dispersion polymerization condition. The effects of the volume ratio of alcohol and water on the morphology of the spherical particles were investigated. There were increasing trends in the particle size with the increasing volume ratio of alcohol and water. Solution polymerization of acrylamide was also studied in the same condition. Linear fit with different feeding ratios of AM and cobalt complex were obtained." @default.
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- W3037665956 date "2020-06-26" @default.
- W3037665956 modified "2023-10-07" @default.
- W3037665956 title "Reversible-deactivation radical polymerizations of acrylamide mediated by cobalt complexes supported by amino-bis(phenolate) ligands" @default.
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- W3037665956 doi "https://doi.org/10.1080/10601325.2019.1691453" @default.
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