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- W3037758020 abstract "A new and practical synthesis of 3-chloro-2,4-difluoro-5-hydroxybenzoic acid, a key intermediate for preparing antimicrobial 3-quinolinecarboxylic acid drugs, is synthesized from 2,4-difluoro-3-chlororobenzoic acid. The protocol involves nitration, esterification, reduction of NO 2 , diazotization, and hydrolysis with a 70% overall yield. The structures of the synthesized compounds are determined by infrared spectroscopy, nuclear magnetic resonance spectroscopy, and high-resolution electrospray ionization mass spectrometry. The advantages of this developed synthetic strategy include an improved overall yield and readily controllable reaction conditions." @default.
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- W3037758020 date "2020-06-23" @default.
- W3037758020 modified "2023-10-15" @default.
- W3037758020 title "A practical synthesis of 3-chloro-2,4-difluoro-5-hydroxybenzoic acid" @default.
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- W3037758020 doi "https://doi.org/10.1177/1747519820932259" @default.
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