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- W3038636705 abstract "Cyclocarbonylative Sonogashira reactions of ortho-ethynylbenzamides have been investigated. The process is carried out under CO pressure, in the presence of a very small amount of PdCl2(PPh3)2 (0.4 mol %) as a catalytic precursor and without the need for a Cu salt as the co-catalyst. 2-Ethynylbenzamide reacted successfully with iodoarenes bearing electron-withdrawing and electron-donating groups, giving rise to different classes of compounds depending on the solvent used. On the contrary, N-(4-chlorophenyl)-2-ethynylbenzamide afforded exclusively polyfunctionalized isoindolinones with high stereoselectivity toward (E) isomers." @default.
- W3038636705 created "2020-07-10" @default.
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- W3038636705 date "2020-07-03" @default.
- W3038636705 modified "2023-10-18" @default.
- W3038636705 title "Synthesis of 3-Alkylideneisoindolin-1-ones via Sonogashira Cyclocarbonylative Reactions of 2-Ethynylbenzamides" @default.
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- W3038636705 doi "https://doi.org/10.1021/acs.joc.0c01282" @default.
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