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- W3038750994 abstract "Silica-based (SiO 2 ) poly(3-hydroxybutyrate) (PHB) nanocomposites were obtained via an in situ sol–gel route in three distinct particle concentrations (1, 5, and 7.5% by weight of PHB). The polymer hybrids formed were analyzed via wide-angle X-ray diffraction (WAXD), small-angle X-ray scattering (SAXS), Fourier transform infrared (FTIR) spectroscopy, and time-domain nuclear magnetic resonance relaxometry (TD-NMR). The SiO 2 inorganic structure displayed surface fractal features at low concentration (1 wt%) and denser agglomerates at higher concentrations (5 and 7.5 wt%). FTIR and SAXS results confirmed the formation of the inorganic matrix amid the polymer chains with different levels of distribution and organization. WAXD and TD-NMR results suggested the SiO 2 influence on the PHB crystallinity degree, which was reflected on the polymer’s molecular dynamics with a nonlinear dependence of particles concentration in the PHB matrix." @default.
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- W3038750994 date "2020-07-03" @default.
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- W3038750994 title "Spectroscopic evidence of successful in situ insertion of sol–gel silica in a poly(3-hydroxybutyrate) matrix" @default.
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- W3038750994 doi "https://doi.org/10.1177/0892705720935939" @default.
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