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- W3039082536 endingPage "156278" @default.
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- W3039082536 abstract "Solid-oxide iron-air batteries have potential for applications in large-scale energy storage systems, but their storage materials, iron and iron oxides, have limited cycle life due to powder sintering and choking of gas flow. To address this issue, Fe foams are synthesized with either equiaxed or directional dendritic pore structures by camphene-based freeze casting of Fe2O3 powders, followed by H2 reduction to Fe and sintering. For each pore architecture, Fe foams are created with three different initial porosities, ranging from 47 to 63 vol %, and are then cycled at 800 °C under alternating oxidation (via H2O) and reduction (via H2) conditions. The redox-cycled foams are examined by optical microscopy, scanning electron microscopy, and synchrotron X-ray tomography to assess the evolution of their porosity driven by the redox volume changes, sintering, and micropore formation via the Kirkendall effect. After 5 redox cycles, the Fe foams have lost the majority (39 ± 2 vol %) of their initial porosity." @default.
- W3039082536 created "2020-07-10" @default.
- W3039082536 creator A5002076591 @default.
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- W3039082536 date "2020-12-01" @default.
- W3039082536 modified "2023-09-25" @default.
- W3039082536 title "Effects of pore morphology on the cyclical oxidation/reduction of iron foams created via camphene-based freeze casting" @default.
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- W3039082536 doi "https://doi.org/10.1016/j.jallcom.2020.156278" @default.
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