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• W3039148532 abstract "Transition-metalarene complexes are important species in catalysisand arene functionalization. Certain electron-rich metal fragmentsare capable of binding arenes across two adjacent carbon atoms, inducingsignificant dearomatization through strong back-bonding interactions.Such complexes generally adopt low-spin, closed-shell configurationswith electronic and coordinative saturation. Herein, we report anasymmetric tris­(pyrazolyl)­hydroborate (Tp) ligand and its Fe­(I) fragment,which forms η2 complexes with a range of arenes andheteroarenes, including benzene, trifluoromethylbenzene, naphthalene,anthracene, and furan. X-band EPR and solution magnetometry definitivelyestablish these complexes as high spin (S = 3/2),owing to the relatively weak ligand field provided by Tp. These compoundsexpand a small but growing family of complexes that feature stronglyback-bonding metal fragments in high-spin configurations." @default.
• W3039148532 created "2020-07-10" @default.
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• W3039148532 date "2020-06-30" @default.
• W3039148532 modified "2023-10-17" @default.
• W3039148532 title "η²-Arene Binding at High-Spin Fe(I) Enabled by a Sterically Accommodating Tris(pyrazolyl)hydroborate Ligand" @default.
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• W3039148532 doi "https://doi.org/10.1021/acs.organomet.0c00340" @default.
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