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• W3039609904 endingPage "125793" @default.
• W3039609904 startingPage "125793" @default.
• W3039609904 abstract "Ferroelectric triglycine sulphate (TGS) single crystals were grown by conventional slow cooling and unidirectional solution growth method below and above its Curie temperature (Tc). The evolution of morphology of TGS crystals during conventional growth method was imaged in an online and in-situ manner using laser shadowgraphy, and the growth rates of the crystals along a, b and c-axis were measured in both the temperature regimes. It was found that the growth rates of crystal grown above Tc was higher than that of the crystal grown below Tc. TGS crystals oriented along [0 1 0] polar direction and having large (0 1 0) habit face were successfully grown below and above its Curie temperature (Tc) by Sankaranarayanan-Ramasamy (SR) unidirectional solution growth method. Time-lapsed photographs of SR growth process were captured at regular interval of time, from where the growth rates of crystals along [0 1 0] direction was computed to be 1.5 and 2.2 mm/day for crystals grown below and above Tc respectively. The growth conditions were optimized and the dimension of the grown crystals were 60 mm length and 15 mm diameter for below Tc and 35 mm length and 15 mm diameter for above Tc. Using shadowgraphy, the buoyancy-driven convective patterns around the growing TGS crystals were imaged and the gradual buildup of this activity with the dimension of the crystal and time of the growth was investigated. Shadowgraphy was also used to map the evolution of morphology of TGS crystals growing below and above Tc, and growth rates along the three main crystallographic directions were computed. Mach-Zehnder interferometry was used to image development of concentration gradient in the crystallizer during growth." @default.
• W3039609904 created "2020-07-10" @default.
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• W3039609904 date "2020-09-01" @default.
• W3039609904 modified "2023-10-16" @default.
• W3039609904 title "TGS crystal growth below and above Curie temperature (Tc)" @default.
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• W3039609904 doi "https://doi.org/10.1016/j.jcrysgro.2020.125793" @default.
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