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- W3040067102 abstract "Lead and bismuth standards for quantitative electron probe microanalysis have always been a problem due to mechanical polishing and surface oxidation upon atmospheric exposure. Some Pb and Bi compounds, such as the selenides and tellurides, can be obtained commercially as solid pieces that are large enough to be mounted as useful standards, but they can also form non-stoichiometric solid solutions. This paper is a description of the initial work done on the testing of some selenides and tellurides to evaluate their usefulness as standards for quantitation. In addition, improved procedures for preparing the Pb and Bi element and compound specimens are being used to reduce surface oxidation. Primarily Pb samples were evaluated here, but the project will be extended in the future to include more Bi materials. Experimental Most specimens were mounted in silver epoxy in multi-element mounts that were repolished according to the description below. Additional specimens of PbTe, PbSe, and Pb were mounted in epoxy for this work." @default.
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- W3040067102 date "2000-08-01" @default.
- W3040067102 modified "2023-09-27" @default.
- W3040067102 title "Useful Lead and Bismuth Standards for Quantitative Electron Probe Microanalysis" @default.
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- W3040067102 doi "https://doi.org/10.1017/s1431927600037168" @default.
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