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- W3040782806 abstract "This research aimed at implementing and validating a method for analysis of pesticide residues in crops. QuEChERS extraction method with PSA purification was used following analyzes by gas chromatography with tandem mass spectrometry in Selected Reaction Monitoring mode. A short run method was successfully developed for the determination of 41 pesticides, confirmed by two precursor-products for each analyte. The calibration curve for each analyte was linear at concentration range from 1 to 500 μg kg−1 with correlation coefficients higher than 0.99, low limits of detection (0.03 − 10.22 μg kg−1) and satisfactory precision. The developed method was used to investigate apples; mangos; strawberries; cucumbers and tomatoes from the Rio de Janeiro Food Distribution Center (CEASA).Most of the targeted pesticides (78%) were below detection limits. Apple and strawberry presented the highest pesticide contamination levels, many of which are not authorized by tthe Brazilian national regulatory agency (ANVISA)." @default.
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- W3040782806 date "2020-07-11" @default.
- W3040782806 modified "2023-09-26" @default.
- W3040782806 title "Multiresidue method for triazines and pyrethroids determination by solid-phase extraction and gas chromatography-tandem mass spectrometry" @default.
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- W3040782806 doi "https://doi.org/10.1080/03601234.2020.1790266" @default.
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