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• W3040872016 abstract "Start-up conditions largely dictate the performance longevity for solid oxide fuel cells (SOFCs). The SOFC anode is typically deposited as NiO-ceramic that is reduced to Ni-ceramic during start-up. Effective reduction is imperative to ensuring that the anode is electrochemically active and able to produce electronic and ionic current; the bi-polar plates (BPP) next to the anode allow the transport of current and gases, via land and channels, respectively. This study investigates a commercial SOFC stack that failed following a typical start-up procedure. The BPP design was found to substantially affect the spatiotemporal dynamics of the anode reduction; Raman spectroscopy detected electrochemically inactive NiO on the anode surface below the BPP land-contacts; X-ray computed tomography (CT) and scanning electron microscopy (SEM) identified associated contrasts in the electrode porosity, confirming the extension of heterogeneous features beyond the anode surface, towards the electrolyte-anode interface. Failure studies such as this are important for improving statistical confidence in commercial SOFCs and ultimately their competitiveness within the mass-market. Moreover, the spatiotemporal information presented here may aid in the development of novel BPP design and improved reduction protocol methods that minimize cell and stack strain, and thus maximize cell longevity." @default.
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• W3040872016 date "2020-07-10" @default.
• W3040872016 modified "2023-09-26" @default.
• W3040872016 title "The Role of Bi-Polar Plate Design and the Start-Up Protocol in the Spatiotemporal Dynamics during Solid Oxide Fuel Cell Anode Reduction" @default.
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• W3040872016 doi "https://doi.org/10.3390/en13143552" @default.
• W3040872016 hasPublicationYear "2020" @default.
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