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- W304313445 abstract "The determination of four impurity elements (Co, Pb, Mo, and Ti) in a zirconium oxide matrix is described. The method is applicable to the analysis of metal samples which have been removed from ingots, strips, bars, or other shapes and which can be converted readily to the oxide. Synthetic standards containing the appropriate alloying constituents must be used for the analysis of Zircaloys. Metal samples are converted to the oxide in a muffle furnace, and a one gram portion of the oxide is mixed with 100 mg of chromic oxide. The mixture is pressed into the sample electrode and excited in the d-c arc. Then the spectra are recorded photographically, measured photometrically, and the calculated relative intensity ratios referred to the appropriate analytical curves to determine the elemental concentrations. (auth)" @default.
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- W304313445 date "1958-06-19" @default.
- W304313445 modified "2023-09-27" @default.
- W304313445 title "THE SPECTROGRAPHIC DETERMINATION OF IMPURITIES IN ZIRCONIUM AND ZIRCALOY USING A CHROMIUM INTERNAL STANDARD" @default.
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