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• W3043136064 endingPage "693" @default.
• W3043136064 startingPage "693" @default.
• W3043136064 abstract "The reduction of graphene oxide (GO) thin films deposited on substrates is crucial to achieve a technologically useful supported graphene material. However, the well-known thermal reduction process cannot be used with thermally unstable substrates (e.g., plastics and paper), in addition photo-reduction methods are expensive and only capable of reducing the external surface. Therefore, solid-state chemical reduction techniques could become a convenient approach for the full thickness reduction of the GO layers supported on thermally unstable substrates. Here, a novel experimental procedure for quantitative reduction of GO films on paper by a green and low-cost chemical reductant (L-ascorbic acid, L-aa) is proposed. The possibility to have an effective mass transport of the reductant inside the swelled GO solid (gel-phase) deposit was ensured by spraying a reductant solution on the GO film and allowing it to reflux in a closed microenvironment at 50 °C. The GO conversion degree to reduced graphene oxide (r-GO) was evaluated by Fourier transform infrared spectroscopy (FT-IR) in attenuated total reflectance (ATR) mode and X-ray Diffraction (XRD). In addition, morphology and wettability of GO deposits, before and after reduction, were confirmed by digital USB microscopy, scanning electron microscopy (SEM), and contact angle measurements. According to these structural characterizations, the proposed method allows a bulky reduction of the coating but leaves to a GO layer at the interface, that is essential for a good coating-substrate adhesion and this special characteristic is useful for industrial exploitation of the material." @default.
• W3043136064 created "2020-07-23" @default.
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• W3043136064 date "2020-07-17" @default.
• W3043136064 modified "2023-10-06" @default.
• W3043136064 title "Green Solid-State Chemical Reduction of Graphene Oxide Supported on a Paper Substrate" @default.
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• W3043136064 doi "https://doi.org/10.3390/coatings10070693" @default.
• W3043136064 hasPublicationYear "2020" @default.
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