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- W3043144828 endingPage "1583" @default.
- W3043144828 startingPage "1576" @default.
- W3043144828 abstract "Abstract Aminoglycosides are a relevant class of antibiotics widely used by medics and veterinaries. There are a variety of reasons that make their determination relevant, such as quality control, environment and food contamination assessment, drug‐release studies, among others. The lack of a chromophore makes aminoglycoside spectrophotometric detection particularly challenging, often requiring derivatization. In this work, an indirect detection method, making use of imidazole as a probe, applying CZE was successfully tested. It did not require derivatization, which simplified the sample preparation. Suitable figures of merit were obtained; recoveries between 95 and 105%, adequate repeatability and precision, correlation coefficients ( r ) above 0.998, and limits of detection (LODs) of 3.2 and 11 mg/L for gentamicin and paromomycin, respectively. As a proof‐of‐concept, it was also applied in a simple controlled release experiment that was well fitted using the Hill equation." @default.
- W3043144828 created "2020-07-23" @default.
- W3043144828 creator A5052494269 @default.
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- W3043144828 creator A5065467975 @default.
- W3043144828 creator A5069624991 @default.
- W3043144828 creator A5089974549 @default.
- W3043144828 date "2020-08-09" @default.
- W3043144828 modified "2023-10-18" @default.
- W3043144828 title "Derivatization‐free determination of aminoglycosides by CZE–UV in pharmaceutical formulations" @default.
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- W3043144828 doi "https://doi.org/10.1002/elps.202000160" @default.
- W3043144828 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/32683725" @default.
- W3043144828 hasPublicationYear "2020" @default.
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