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• W3044207956 abstract "In most applications,electrocatalysts exhibit a large surface area to volume ratio, for exampleusing nanoparticles. To fully understand fundamental electrochemical processesat the length scale of these nanoparticles, it is necessary to use specializedexperimental techniques. In this thesis, the stability and activity of platinumelectrode surfaces are studied at the nano- and micrometer scale usingElectrochemical Scanning Probe Microscopy (EC-SPM) techniques. Chapters 2 and 3 describe the roughening of an atomically flat Pt(111) surfaceupon repetitive oxidation and reduction. These data were acquired using acombination of Electrochemical Scanning Tunneling Microscopy (EC-STM) andCyclic Voltammetry (CV). Chapter 4 describes the development of a new techniqueto resolve small differences in local reactivity: voltammetric ScanningElectrochemical Cell Microscopy (SECCM). The power of this technique is demonstratedby studying the reactivity of a polycrystalline Pt sample towards hydrazineoxidation. Finally, Chapter 5 compares the reactivity of small Ptultramicroelectrodes to that of conventional macroelectrodes." @default.
• W3044207956 created "2020-07-29" @default.
• W3044207956 creator A5011239656 @default.
• W3044207956 date "2018-11-29" @default.
• W3044207956 modified "2023-09-27" @default.
• W3044207956 title "Platinum electrochemistry through a magnifying glass" @default.
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• W3044207956 hasPublicationYear "2018" @default.
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