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- W3044295439 abstract "Accurate determination of electrode overpotentials is essential to assess the performance of the electrode and understand the rate-limiting steps involved. Three-electrode configuration with the use of a reference electrode at a fixed potential is a standard way to measure overpotential of a specific electrode in liquid electrochemical systems. However, application of such three-electrode configuration to solid electrochemical cells for overpotential determination is not straightforward and requires extra caution. Here we report a theoretical Finite Element Analysis on the geometrical requirements for which the reference electrode can be applied to anode- or electrolyte-supported solid oxide button cells. The modeling results suggest that the symmetry of the working and counter electrodes is the key factor determining if a reference electrode is suitable to use. For anode-supported fuel cells with asymmetrical working and counter electrodes, reference electrode cannot be used under all circumstances. To use reference electrode for overpotential measurements, electrolyte-supported cells with symmetrical semicircular-shaped electrodes are preferred. A data processing procedure has also been presented to obtain the electrode overpotential from the measured potential using the three-electrode scheme in solid oxide electrochemical cells." @default.
- W3044295439 created "2020-07-29" @default.
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- W3044295439 date "2020-01-09" @default.
- W3044295439 modified "2023-09-28" @default.
- W3044295439 title "Precautions of Using Three-Electrode Configuration to Measure Electrode Overpotential in Solid Oxide Electrochemical Cells: Insights from Finite Element Modeling" @default.
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- W3044295439 doi "https://doi.org/10.1149/1945-7111/aba876" @default.
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