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- W3044594889 abstract "A mild process using a combination of TMSCl and NaI in acetonitrile is used to regenerate carbonyl compounds from a variety of dithiane and dithiolane derivatives. This easy to handle and inexpensive protocol is also efficient to deprotect oxygenated and mixed acetals as 1,3‐dioxanes, 1,3‐dioxolanes and 1,3‐oxathianes quantitatively. As a possible extension of this method, it was also shown that nitrogenated substrates such as hydrazones, N ‐tosylhydrazones, and ketimines reacted well under these conditions to give the expected ketones in high yields. The methodology proposed herein is a good alternative to the existing methods since it does not use metals, oxidants, reducing agents, acidic or basic media, and keto‐products were obtained in high to excellent yields." @default.
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- W3044594889 date "2020-08-12" @default.
- W3044594889 modified "2023-10-15" @default.
- W3044594889 title "Mild Deprotection of Dithioacetals by TMSCl/NaI Association in CH<sub>3</sub>CN" @default.
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- W3044594889 doi "https://doi.org/10.1002/ejoc.202000979" @default.
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