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- W3044991023 endingPage "105317" @default.
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- W3044991023 abstract "In this work, poly(ethylene glycol dimethacrylate-N-methacryloyl-L-tryptophan methyl ester) [poly(EGDMA-MATrp)] microbeads (average diameter = 106–300 µm), were synthesized by suspension polymerization technique. The microbeads showed strong affinity and allowed for solid phase extraction (SPE) of two common pesticides; pirimicarb and propoxur in environmental water samples. Some SPE process parameters such as the desorption solvent type, solvent volume, pH and salt concentration were optimized. When it was coupled with high pressure liquid chromatography (HPLC-PDA) for the determination of analytes, the linear ranges were about 10–800 ng mL−1 and the detection limits were 0.95–2.85 ng mL−1. Also the correlation coefficients (0.9949–0.9991) and precisions (2.15–2.52% RSD, n = 3) were determined. The technique was also applied to the enrichment of these pesticides in various environmental water samples. However, no target analyte was detected in the samples. Therefore, samples were spiked and recovery values were obtained in the range of 95.8–104.2% with RSDs of 2.6–6.6%." @default.
- W3044991023 created "2020-07-29" @default.
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- W3044991023 date "2020-11-01" @default.
- W3044991023 modified "2023-10-14" @default.
- W3044991023 title "Development of a new solid phase extraction method for sensitive determination of some carbamate pesticides in water using poly(EGDMA-MATrp) microbeads" @default.
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- W3044991023 doi "https://doi.org/10.1016/j.microc.2020.105317" @default.
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