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- W3045785266 abstract "The amount of β-1 structures in lignin is small; however, they are assumed to significantly affect the reactivity of lignin because they form dienone structures. A method employing thioacidolysis and subsequent desulfurization yields products that can be analyzed via gas chromatography–mass spectrometry (GC–MS) to quantify these β-1 structures. However, the retention times and response factors of the reaction products have not been accurately determined thus far. Here, 12 standard compounds combined with p-hydroxyphenyl (H), guaiacyl (G), and syringyl (S) units were synthesized, and their retention times and response factors were determined through GC–MS, using selective ions. Based on these data, we also investigated the β-1 structures of lignocellulosic lignin samples. Our results clarified that the successful formation of the β-1 structure was dependent on the type of aromatic rings present; there were very few β-1 structures containing H units; and the amount of G–G type was higher and that of the heterotype, i.e., G–S type, was lower than the stochastic value." @default.
- W3045785266 created "2020-08-03" @default.
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- W3045785266 date "2020-07-28" @default.
- W3045785266 modified "2023-10-14" @default.
- W3045785266 title "Combinations of the Aromatic Rings in β-1 Structure Formation of Lignin Based on Quantitative Analysis by Thioacidolysis" @default.
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- W3045785266 doi "https://doi.org/10.1021/acs.jafc.0c03206" @default.
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