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- W3046151010 abstract "Abstract Barium carbonate (BaCO3) nanocrystals were synthesized at ∼20 °C by Chemical Bath Deposition technique in the absence of additives. Chemical kinetic mechanism analysis is presented to understand the formation of the BaCO3 nanocrystal associated with the Ba2+ and C O 3 2 - ions. The BaCO3 nanocrystals were thermally annealing treated at ∼500 °C (BaCO3-TT) and the corresponding thermal effects on morphology, grain size, dislocation density (δ), and crystalline phase, were studied. We identified javelin-like, quasi-spherical, and rod-like complex nanostructures by Scanning Electron Microscopy (SEM). We found that the thermal annealing treatment produces a drastic change in morphology, presenting change to dendrite-like complex nanostructures. The FTIR spectra were recorded, both BaCO3 and BaCO3-TT exhibit the same frequency absorptions bands. Those bands at ∼855 cm−1, ∼693 cm−1, and ∼1090 cm-1 are assigned to out-of-plane bending vibrations of C O 3 2 - ion while the frequency absorption band at ∼1411 cm-1 is connected with the asymmetric stretching vibration of C O 3 2 - ion. BaCO3 powders have a rhombohedral crystalline phase, maintaining this crystalline phase even with thermal annealing treatment, confirming the thermal stability of this material. The calculated strain values ∼2.141 × 10-3 and ∼1.15 × 10-3, and the dislocation density ∼1.15 × 10-3 lines m-2 and ∼2.29 × 1015 lines m-2 justify the observed crystalline defects of BaCO3 and BaCO3-TT nanocrystals." @default.
- W3046151010 created "2020-08-03" @default.
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- W3046151010 date "2020-11-01" @default.
- W3046151010 modified "2023-09-26" @default.
- W3046151010 title "Javelin-like, quasi-spherical, dendrite-like and rod-like complex nanostructures of BaCO3 growth by chemical bath deposition technique" @default.
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- W3046151010 doi "https://doi.org/10.1016/j.ijleo.2020.165316" @default.
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