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- W3046318978 abstract "Abstract Acetylene carbon black has excellent conductivity, structural assortment and adsorption characteristics. To the best of our knowledge, this is the first time that carbon black has been used for assembling regenerable electrochemiluminescence (ECL) sensors. The present method involves the immobilization of Ru(phen) 3 2+ on acetylene carbon black without using any ionic exchanger, owing to the strong adsorption capability of acetylene carbon black toward Ru(phen) 3 2+ , thereby avoiding the loss of activity resulting from the migration of ruthenium complex into the hydrophobic region of ionic exchanger. The developed Ru(phen) 3 2+ ‐acetylene carbon black regenerable ECL sensor for the determination of oxalate shows a linear response from 1×10 −7 M to 1×10 −3 M with a remarkable detection limit of 2.5×10 −9 M (S/N=3). The effect of various commonly associated species within real samples was also explored. The proposed method was successfully applied for the determination of oxalate in urine samples. The as‐prepared Ru(phen) 3 2+ ‐acetylene carbon black regenerable ECL sensor exhibits outstanding long‐term stability over six months and also good reproducibility. The relative standard deviation of five repeated values of 1.0 mM oxalate concentrations is 4.1 %. The developed Ru(phen) 3 2+ ‐acetylene carbon black regenerable ECL sensor is promising for ECL detection." @default.
- W3046318978 created "2020-08-07" @default.
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- W3046318978 date "2020-08-20" @default.
- W3046318978 modified "2023-10-13" @default.
- W3046318978 title "Immobilization of Tris(1,10‐phenanthroline)ruthenium on Acetylene Carbon Black for Regenerable Electrochemiluminescence Sensors Free from Ionic Exchanger" @default.
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- W3046318978 doi "https://doi.org/10.1002/celc.202000904" @default.
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