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- W3047269743 abstract "Abstract Benzoxazine resins have attracted much attention because of their excellent properties. As a new kind of thermosetting resin, their gelation and vitrification behaviors during the curing process are worth studying for promoting their development, but few research works have been done on this subject. In this work, an ordinary diamine‐type benzoxazine resin (PH‐ddm) was chosen as a research object. Its curing kinetics were studied by differential scanning calorimetry (DSC) and a phenomenological model was used to get equal curing degree curves reflecting the relationship among curing degree, curing temperature and time. Moreover, a gelation curve and a vitrification curve of PH‐ddm based on an Arrhenius equation and a DiBenedetto equation were obtained by parallel plate rheometer and modulated DSC (MDSC), respectively. Then, a well‐known time–temperature–transformation (TTT) diagram was plotted. Besides, the rheological behavior of PH‐ddm was analyzed through rotatory viscometer testing and modified double Arrhenius equation to obtain the equal viscosity curves. A TTT–viscosity diagram was obtained through combining the equal viscosity curves with the TTT diagram. This is the first time for using the TTT diagram to investigate the curing process of benzoxazine resins. Our results provide an effective method to optimizing molding conditions of the benzoxazine resins." @default.
- W3047269743 created "2020-08-10" @default.
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- W3047269743 date "2020-08-04" @default.
- W3047269743 modified "2023-10-01" @default.
- W3047269743 title "Time–temperature–transformation (TTT) and TTT–viscosity diagrams of a typical benzoxazine resin" @default.
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- W3047269743 doi "https://doi.org/10.1002/app.49737" @default.
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