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• W3047905602 abstract "The reaction of the equimolar ratio of ammonium pyrrolidinedithiocarbamate {(NH4)PyDT} and sodium N,N-diethyldithiocarbamate (NaEt2DT) with the divalent ion salts of zinc, cadmium and mercury resulted in the complexes of the type [M(κ2-PyDT)(κ2-Et2DT)]; {M(II) = Zn, Cd, Hg}. These complexes were characterized using different techniques: elemental analysis, molar conductivity, FTIR, 1H NMR, 13C{1H} NMR and HSQC. The results demonstrate the bidentate chelating mode of the two dithiocarbamate ligands through the sulfur atoms to afford a tetrahedral geometry around the metal ion. Surprisingly, these coordination compounds were obtained as nanocomplexes with regular geometrical nanostructures as follows; [Zn(κ2-PyDT)(κ2-Et2DT)] (1) as nanosheets with a thickness of 21–24 nm, [Cd(κ2-PyDT)(κ2-Et2DT)] (2) as nanorods with a diameter of 70–380 nm while [Hg(κ2-PyDT)(κ2-Et2DT)] (3) was found as merged nanospheres with a diameter of 54–70 nm. These nanostructures have been demonstrated using the SEM and X-ray diffraction of the powder." @default.
• W3047905602 created "2020-08-13" @default.
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• W3047905602 date "2021-01-01" @default.
• W3047905602 modified "2023-10-16" @default.
• W3047905602 title "Novel dithiocabamate nano Zn(II), Cd(II) and Hg(II) complexes with pyrrolidinedithiocarbamate and N,N-diethyldithiocarbamate" @default.
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• W3047905602 doi "https://doi.org/10.1016/j.matpr.2020.07.082" @default.
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