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• W3048239235 abstract "A 12-step asymmetric synthesis of thromboxane B2 (TxB2) from 2,5-dimethoxytetrahydrofuran is described. The synthesis employs our organocatalytic aldol reaction of succinaldehyde to give a key bicyclic enal intermediate. From here, the synthetic strategy involves a conjugate addition of an alkenyl side chain to the bicyclic enal, Baeyer–Villiger oxidation, and a highly Z-selective Wittig olefination of a hemiacetal. Key to success was minimizing redox operations and the manipulation of functional groups in the correct order." @default.
• W3048239235 created "2020-08-13" @default.
• W3048239235 creator A5016437961 @default.
• W3048239235 creator A5078544922 @default.
• W3048239235 date "2020-08-07" @default.
• W3048239235 modified "2023-10-15" @default.
• W3048239235 title "Total Synthesis of Thromboxane B₂ via a Key Bicyclic Enal Intermediate" @default.
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• W3048239235 doi "https://doi.org/10.1021/acs.orglett.0c02299" @default.
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