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- W3048457850 endingPage "116827" @default.
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- W3048457850 abstract "To better understand the system and conversion of cellulose allomorphs, cellulose III nanocrystals (CNC-III) were used to investigate the crystalline stability of cellulose III in the hydrothermal condition and a lower concentrated NaOH-water system. It was shown that H2O or alkali played an important role in the process of polymorphic transformation. The CNC-III allomorph turned back to cellulose I with an extremely low crystallinity (∼4.18 %) during hydrothermal process at 90-95 °C, or cellulose II when the temperature excessed boiling point (≥100 °C). Furthermore, CNC-III could be rapidly dissolved in an aqueous NaOH (∼7 wt.%) without a pre-cooled treatment to obtain its stable solution. Afterwards, cellulose II with a steady average crystallite size (∼34) was acquired after the regeneration process via dialysis with distilled water. The polymorphic transformation was also analyzed by X-ray diffraction (XRD), solid-state 13C nuclear magnetic resonance (13C NMR)." @default.
- W3048457850 created "2020-08-18" @default.
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- W3048457850 date "2020-12-01" @default.
- W3048457850 modified "2023-09-25" @default.
- W3048457850 title "Crystalline stability of cellulose III nanocrystals in the hydrothermal treatment and NaOH solution" @default.
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- W3048457850 doi "https://doi.org/10.1016/j.carbpol.2020.116827" @default.
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