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• W3048588834 endingPage "105410" @default.
• W3048588834 startingPage "105410" @default.
• W3048588834 abstract "Abstract Series of sorbents, N-sulfonyl-4-hydroxymethyl-1,2,3-triazole functionalized SBA-15 (x-S-SO2-triazole-OH; x=5 -20 wt.%), have been developed via a two-step synthesis strategy: first, co-condensation of 6-azidosulfonylhexyltriethoxysilane and tetraethoxysilane to form 6-azidosulfonylhexyl functionalized SBA-15; and second, the Click reaction of 6-azidosulfonylhexyl functionalized SBA-15 with propyn-1-ol to form (x-S-SO2- triazole-OH). The sorbents with abundant hydrogen bonding sites were used in a stir bar-supported micro-solid-phase extraction (SB-μ-SPE) for six selected phenolic compounds in 10 mL water samples, and the 20-S-SO2-triazole-OH sorbent presented the best extraction efficiency. The linearity range for all tested phenols is within 1 – 1000 ng mL-1 with R value up to 0.9931 and a detection limit (LOD) of 0.03 – 0.30 ng mL-1. The RSD values were determined in the range of 2 – 16% and the relative recoveries in the domestic wastewater sample successfully presented a range of 84.5–108.6%." @default.
• W3048588834 created "2020-08-18" @default.
• W3048588834 creator A5021424377 @default.
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• W3048588834 date "2020-12-01" @default.
• W3048588834 modified "2023-09-26" @default.
• W3048588834 title "N-sulfonyl-4-hydroxymethyl-1,2,3-triazole functionalized SBA-15: A porous organic-inorganic material for trace-level phenolic compounds extraction from water samples by stir bar-supported micro-solid-phase extraction" @default.
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• W3048588834 doi "https://doi.org/10.1016/j.microc.2020.105410" @default.
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