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• W3048653905 abstract "Abstract The dynamic covalent self‐assembly of 14 units of bis(perfluorocatecholato)silane leads to [Si(O 2 C 6 F 4 ) 2 ] 14 —the first giant perfluorinated macrocycle. The oligomerization process is monitored spectroscopically, and the macrocycle analyzed by single‐crystal X‐ray diffraction. The molecule forms a rigid cavity that can host two o ‐closo‐dodecacarboranes. Computations rationalize the consistent and reproducible formation of the 14mer and disclose a non‐catalyzed Si−O/ Si−O σ‐bond metathesis with an exceptionally low energetic barrier. For the first time, the most prevalent linker in our geosphere‐SiO 4 ‐is disposed to construct a shape‐defined crystalline macromolecule." @default.
• W3048653905 created "2020-08-18" @default.
• W3048653905 creator A5000849314 @default.
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• W3048653905 date "2020-10-02" @default.
• W3048653905 modified "2023-10-05" @default.
• W3048653905 title "[Si(O ₂ C ₆ F ₄ ) ₂ ] ₁₄ : Self‐Assembly of a Giant Perfluorinated Macrocyclic Host by Low‐Barrier Si−O Bond Metathesis" @default.
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• W3048653905 doi "https://doi.org/10.1002/anie.202009942" @default.
• W3048653905 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/7756369" @default.
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• W3048653905 hasPublicationYear "2020" @default.
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