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- W3058479460 abstract "Generation of zero-dimensional molybdenum disulphide (MoS 2 ) nanoparticles with effective chemical and physical properties have offered a widerange of applications. The advancement in two-dimensional (2D) MoS 2 functionalization materials for the fabrication of biomedical applications has become a recent trend owing to their physicochemical properties such as high surface area, mechanical properties, and excellent electrical conductivity. In this study, the pristine bulk MoS 2 was exfoliated by probe sonication with glutathione (GSH) as a capping ligand to form MoS 2 -GSH nanoparticles. Further, the as-prepared MoS 2 -GSH was coated with amino terminated ethyl polyethylene glycol (MoS 2 -GSH-AEPEG) through electrostatic interactions between GSH and AEPEG. Thereafter, both MoS 2 -GSH and MoS 2 -GSH-AEPEG nanoparticles (NPs) were chelated with manganese (Mn) metal ion to form magnetic MoS 2 -GSH-Mn and MoS 2 -GSH-AEPEG-Mn NPs. The obtained MoS 2 -GSH-Mn and MoS 2 -GSH-AEPEG-Mn nanoparticles exhibited a spherical in shape with sizes of 60.7 and 80.6 nm, respectively. The chelated Mn 2+ in the prepared MoS 2 NPs was confirmed by XPS and Raman spectroscopy. The paramagnetic properties of the MoS 2 -GSH-Mn and MoS 2 -GSH-AEPEG-Mn samples were investigated using a superconducting quantum interference device at 5 K temperature and the saturation magnetization was calculated to be 17.5 and 15 emu/g for MoS 2 -GSH-Mn and MoS 2 -GSH-AEPEG-Mn, respectively. The MoS 2 -GSH-Mn exhibited higher magnetic hysteresis loops than MoS 2 -GSH-AEPEG-Mn due to shielding effects of nonmagnetic nature of PEG coating." @default.
- W3058479460 created "2020-08-24" @default.
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- W3058479460 date "2021-01-01" @default.
- W3058479460 modified "2023-09-24" @default.
- W3058479460 title "Paramagnetic properties of manganese chelated on glutathione-exfoliated MoS2" @default.
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- W3058479460 doi "https://doi.org/10.1016/j.colsurfa.2020.125432" @default.
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