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- W3074164611 abstract "Chloroformylation reactions are versatile reactions that allow the introduction of a chlorine atom and an aldehyde group in enolizable ketones, employing the well-known Vilsmeier reagent. However, the use of this unstable reagent is usually associated with hazards, especially when it is used on an industrial scale. The present article describes the preparation and use of the Vilsmeier reagent under continuous flow conditions for the preparation of an important intermediate in the synthesis of cyanine dyes. In addition, the traditionally used dimethylformamide has been substituted with more desirable formamides, together with the removal of the halogenated solvent usually employed in the reaction. Consequently, the optimized conditions allow the continuous production of the target compound in a 79–81% isolated yield in a more environmentally friendly, fast, and secure manner." @default.
- W3074164611 created "2020-08-24" @default.
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- W3074164611 date "2020-08-17" @default.
- W3074164611 modified "2023-10-13" @default.
- W3074164611 title "A Vilsmeier Chloroformylation by Continuous Flow Chemistry" @default.
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- W3074164611 doi "https://doi.org/10.1021/acs.oprd.0c00318" @default.
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