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- W3081314882 abstract "Abstract A facile preparation of 3-hydroxylisoquinolin-1, 4-diones and piperidine-2,5-dione from alkyne-tethered amide is reported under cerium photocatalysis and O2 balloon. The reaction works well with a broad reaction scope and reaction efficiency. Mechanism studies indicate that 3-hydroxylpyrrolidin-2-one-containing α-ketol radical species serves as a possible key intermediate, and the final product is attributed to a formal N-centered radical initiated [2 + 2] cyclization and α-ketol rearrangement. Interestingly, divergence towards C N bond migration and C C bond migration is reached in this radical α-ketol rearrangement." @default.
- W3081314882 created "2020-09-01" @default.
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- W3081314882 date "2020-11-01" @default.
- W3081314882 modified "2023-10-17" @default.
- W3081314882 title "Preparation of 3-hydroxyisoquinoline-1,4-dione and piperidine-2,5-dione under cerium photocatalysis from alkyne-tethered N-alkoxylamide with O2" @default.
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- W3081314882 doi "https://doi.org/10.1016/j.mcat.2020.111163" @default.
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