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- W3082860151 abstract "High-entropy aluminum garnets were grown as bulk single crystals using the micro-pulling-down method, taking the synthesis of complex ceramics a step further from the conventional preparation of polycrystalline materials. We studied the effects of growth parameters on the elemental distribution in high optical quality crystals of (Lu1/6Y1/6Ho1/6Dy1/6Tb1/6Gd1/6)3Al5O12 containing six cations (yttrium and rare-earths) taken in equimolar amounts. A single garnet structure was confirmed by powder X-ray diffraction. Electron microprobe measurements were obtained to correlate the radial distribution of rare-earth elements with pulling rates and molten zone height. The nature of the elemental distribution in the radial direction was associated with ionic radius: smaller rare-earths concentrated in the center of the crystal, while larger rare-earths segregated toward the outer edge of the cylindrical crystal. Faster pulling rates led to a flattening of the concentration profiles toward the nominal concentration, promoting a more homogeneous radial elemental distribution, while varying the molten zone height did not have a significant effect. The demonstrated success with crystal growth enables the practical availability of single crystals of multicomponent aluminum garnets for further discovery of new phenomena and applications." @default.
- W3082860151 created "2020-09-08" @default.
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- W3082860151 date "2020-09-02" @default.
- W3082860151 modified "2023-10-06" @default.
- W3082860151 title "Crystal Growth and Elemental Homogeneity of the Multicomponent Rare-Earth Garnet (Lu<sub>1/6</sub>Y<sub>1/6</sub>Ho<sub>1/6</sub>Dy<sub>1/6</sub>Tb<sub>1/6</sub>Gd<sub>1/6</sub>)<sub>3</sub>Al<sub>5</sub>O<sub>12</sub>" @default.
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- W3082860151 doi "https://doi.org/10.1021/acs.cgd.0c00887" @default.
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