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- W3083079076 abstract "In this study, a novel energetic compound 3-nitro-1-(2 H -tetrazol-5-yl)-1 H -pyrazole-4-carboxylic acid ( 1 ) and a series of corresponding energetic salts ( 2 – 4 ) were designed and synthesized. Their chemical structures were determined through NMR spectra, elemental analysis, FT-IR, and single crystal X-ray diffraction. All of these energetic compounds displayed low sensitivity to impact (IS > 40 J) and friction (FS > 240 N) and acceptable detonation properties. Compound 1 – 3 showed high thermal stability, with decomposition temperatures higher than 300 °C. In addition, the structure–property relationship of these compounds was elucidated by crystal stacking analyses combined with energetic performance parameters. In this way, a new approach for the development of novel energetic materials can be provided given the high performance of these energetic compounds. A novel 5-(1H-pyrazol-1-yl)-2H-tetrazole backbone with planar structure and corresponding energetic salts based on potassium, hydroxylammonium, and hydrazinium were readily obtained through acid-base reactions. Those energetic compounds have high thermal stability and low mechanical sensitivity." @default.
- W3083079076 created "2020-09-11" @default.
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- W3083079076 date "2020-09-01" @default.
- W3083079076 modified "2023-10-18" @default.
- W3083079076 title "Synthesis of 5-(1H-pyrazol-1-yl)-2H-tetrazole-derived energetic salts with high thermal stability and low sensitivity" @default.
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- W3083079076 doi "https://doi.org/10.1016/j.enmf.2020.08.004" @default.
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