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• W3083890931 abstract "A modified QuEChERS method was employed with LC-MS/MS to evaluate the matrix effects of 12 different vegetables matrices in 57 globally used herbicides. The average recoveries of pesticides at different concentrations varied between 70 and 120%. The reproducibility expressed as relative standard deviation was <25%. The limit of quantitation was (0.005–0.01 mg/kg). The measurement uncertainty is lower than 40%. Three vegetables families: Cucurbitaceae, Solanaceae and leafy vegetables were selectd for study. Among the investigated commodities, leafy green vegetables have the highest matrix effects, MEs percentages ranged between (2 & 282%). The highest suppression in analytes response was observed for parsley with matrix ME (2–19%). Most of tested herbicides showed suppression extent at the lower fortified concentrations. Tomato recorded the highest enhancement in most of studied herbicides of MEs% ranged from (122 to 379%). Butachlor, chlorbromuron, fenoxaprop-p-ethyl, flufenacet, fluzafop-p-butyl, hexythiazox, prosulfocarb and pyriproxyfen showed ion suppresion for all vegetables matrices with MEs% ranged from (5 to 79%). Matrix effects (MEs) were evaluated by comparing the slopes of target analytes to prove reproducibility (n = 5). The current study emphasize using of matrix match calibration with these commodity pesticides combinations, whereas, ME’s were dependent on composition of analyte and co-eluting agents." @default.
• W3083890931 created "2020-09-14" @default.
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• W3083890931 date "2020-01-01" @default.
• W3083890931 modified "2023-09-27" @default.
• W3083890931 title "Evaluation of method performance and matrix effect for 57 commonly used herbicides in some vegetable families using LC-MS/MS determination" @default.
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• W3083890931 doi "https://doi.org/10.1080/23311932.2020.1815287" @default.
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