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- W3083892013 abstract "The advanced organic chemistry experiments describe the preparation of fused six-membered lactams to isoxazole and isoxazoline by employing Ugi four-component reaction (U-4CR) and intramolecular nitrile oxide cyclization (INOC) synthetic sequence. The experiments were carried out in 28 h (overnight for U-4CR) and 2 h (for INOC) using commercially available starting materials. The two-step reaction involves the in situ imine formation in the one-pot multicomponent reaction and in situ nitrile oxide formation in the INOC. The experiments are useful in the organic chemistry curriculum for the introduction of a one-pot multicomponent reaction and 1,3-dipolar cycloaddition reactions." @default.
- W3083892013 created "2020-09-14" @default.
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- W3083892013 date "2020-09-08" @default.
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- W3083892013 title "Synthesis of Fused Six-Membered Lactams to Isoxazole and Isoxazoline by Sequential Ugi Four-Component Reaction and Intramolecular Nitrile Oxide Cyclization" @default.
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- W3083892013 doi "https://doi.org/10.1021/acs.jchemed.9b01169" @default.
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