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- W3086377675 abstract "Supported catalytically active liquid metal solutions have been receiving increasing attention recently. We investigated the oxidation behavior of macroscopic Rh–Ga alloy droplets and Rh–Ga model catalyst nanoparticles supported on SiO2/Si(100) with low Rh content (<2.5 at. %) by x-ray photoelectron spectroscopy in ultra-high vacuum and under near-ambient pressure conditions using different photon energies and also using transmission electron microscopy. The experiments are accompanied by computational studies on the Ga oxide/Rh–Ga interface and Rh–Ga intermetallic compounds. For both Rh–Ga alloy droplets and Rh–Ga model catalyst nanoparticles, exposure to molecular oxygen leads to the formation of an oxide shell in which Rh is enriched. Transmission electron microscopy on the Rh–Ga nanoparticles confirms the formation of an ∼4 nm thick gallium oxide film containing Rh. Based on ab initio molecular dynamics and computational studies on the Ga2O3/Ga interface, it is concluded that Rh incorporation into the Ga2O3 film occurs by substituting octahedrally coordinated Ga." @default.
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- W3086377675 date "2020-09-11" @default.
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- W3086377675 title "Oxidation induced restructuring of Rh–Ga SCALMS model catalyst systems" @default.
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- W3086377675 doi "https://doi.org/10.1063/5.0021647" @default.
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