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• W3088391322 endingPage "119871" @default.
• W3088391322 startingPage "119871" @default.
• W3088391322 abstract "During pharmaceutical manufacturing, line-scan hyperspectral imaging enables us to collect several electromagnetic spectra at each pixel in a two-dimensional plane for each tablet. The present study quantitatively determines two independent values of the active pharmaceutical ingredient (API) content in a tablet and the amount of coating on a surface of the same tablet simultaneously; the process is visualized by means of a near-infrared hyperspectral imaging (NIR-HSI) system combined with multivariate data analysis at a typical manufacturing speed of 4,000 tablets per minute. The API content and the amount of coating were controlled to be in the range 80–120% and 0–7 mg, respectively. The results of the cross validation of regression models demonstrated a coefficient of determination (R2) of 0.942, a root-mean-square error of cross validation (RMSECV) of 3.48% for the API content, an R2 of 0.939, and an RMSECV of 0.46 mg for the amount of coating. These results demonstrated that the API content in a tablet as well as the amount of coating on the surface of the same tablet can be simultaneously determined with sufficient accuracy. This technique is practically applicable to process analytical technology in pharmaceutical manufacturing." @default.
• W3088391322 created "2020-10-01" @default.
• W3088391322 creator A5017531694 @default.
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• W3088391322 date "2020-11-01" @default.
• W3088391322 modified "2023-09-30" @default.
• W3088391322 title "Real-time determination and visualization of two independent quantities during a manufacturing process of pharmaceutical tablets by near-infrared hyperspectral imaging combined with multivariate analysis" @default.
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• W3088391322 doi "https://doi.org/10.1016/j.ijpharm.2020.119871" @default.
• W3088391322 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/32980509" @default.
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