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- W3088764209 abstract "Oxidative addition of the C2–X (X = Cl, Br) bond of 2‐halogenopyridines or 2‐chloroquinoline to zero‐valent group 10 metal complexes in the presence of a proton source leads to complexes bearing pyridine‐derived protic remote NHC ( r NHC) ligands. The oxidative addition of 2‐halogeno‐functionalized pyridine derivatives to complexes [M 0 (PPh 3 ) 4 ] (M = Pd, Pt) in the presence of NH 4 BF 4 or NH 4 PF 6 yielded complexes trans ‐[ 1 ]PF 6 – trans ‐[ 5 ]BF 4 with a trans ‐arrangement of the two remaining PPh 3 ligands. The oxidative addition to Ni 0 was achieved by reaction of the halogenopyridine derivatives with [Ni(cod) 2 ]/PEt 3 in the presence of a proton acid (NH 4 BF 4 or NH 4 PF 6 ) yielding complexes of type trans ‐[Ni(protic‐ r NHC)(PEt 3 ) 2 X]A (A = BF 4 – , PF 6 – ). In the absence of a proton source, the oxidative addition of 2‐chloroquinone to [Ni(cod) 2 ]/PEt 3 yielded the neutral complex trans ‐[ 8 ] bearing an anionic quinoline‐derived r NHC ligand. The molecular structures of selected complexes have been determined by X‐ray diffraction studies." @default.
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- W3088764209 date "2020-10-06" @default.
- W3088764209 modified "2023-09-26" @default.
- W3088764209 title "Oxidative Addition of 2‐Halogenopyridines and 2‐Chloroquinoline to Zero‐Valent Group 10 Metals" @default.
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- W3088764209 doi "https://doi.org/10.1002/zaac.202000279" @default.
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