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• W3089601907 abstract "Vanadium carbide is known, for its hardness and other unique properties, as a refractory material. The synthesis of vanadium carbide is always associated with the utilization of expensive active metals, such as aluminum, calcium and magnesium, as a reducing agent to extract the vanadium metal from its corresponding oxide, followed by carbidization. The carbidization of reduced vanadium requires a complicated process and elevated temperature. Mechanical activation to synthesize vanadium carbide from its corresponding oxide and carbon source represents a promising, straightforward and less energy-intensive route. In the present study, vanadium carbide is synthesized by the carbothermic reduction of a mechanically activated mixture of V2O5 and carbon black as reducing agents without any additives. The reduction process is monitored by means of thermogravimetric analysis. The reduction products are characterized by X-ray diffraction and field emission scanning electron microscope. It is found that V8C7 with an average crystallite size of 88 nm can be synthesized from a V2O5-C mixture after milling for 15 h and further heating at 1050 °C for 1 h in an inert atmosphere." @default.
• W3089601907 created "2020-10-08" @default.
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• W3089601907 date "2020-10-02" @default.
• W3089601907 modified "2023-10-17" @default.
• W3089601907 title "Synthesis of Vanadium Carbide by Mechanical Activation Assisted Carbothermic Reduction" @default.
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• W3089601907 doi "https://doi.org/10.3390/ma13194408" @default.
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