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- W3089944105 abstract "In advancing host-guest (H-G) chemistry, considerable effort has been spent to synthesize host molecules with specific and well-defined molecular recognition characteristics including selectivity and adjustable affinity. An important step in the process is the characterization of binding strengths of the H-G complexes. This characterization is typically performed in solution using NMR or fluorescence. Gas-phase investigation of energetics of H-G systems is of great importance in providing information regarding their intrinsic binding properties. The major portion of this thesis is devoted to the study of the energetics of H-G complexes formed by three hemicryptophane cage hosts with various biologically-relevant guest molecules. Among the existing tandem mass spectrometry-based techniques, here we employ blackbody infrared radiative dissociation (BIRD), low-energy collision induced dissociation (low-energy CID), higher-energy collision dissociation (HCD) and high-pressure CID for measurements of energetics of H-G complexes. These techniques were used either alone, or in combination with each other, or with Rice–Ramsperger–Kassel–Marcus (RRKM) modeling. This work has allowed us to develop the low-energy CID, a promising technique, but so far infrequently used." @default.
- W3089944105 created "2020-10-08" @default.
- W3089944105 creator A5029577353 @default.
- W3089944105 date "2018-09-28" @default.
- W3089944105 modified "2023-09-26" @default.
- W3089944105 title "Tandem mass spectrometry for investigation of binding energies of host-guest complexes and structural elucidation of oligosaccharides" @default.
- W3089944105 hasPublicationYear "2018" @default.
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