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• W3092844982 abstract "The phase diagram and melting behavior of the equimolar water–ammonia mixture have been investigated by Raman spectroscopy, x-ray diffraction, and visual observations from 295 K to 675 K and up to 9 GPa. Our results show non-congruent melting behavior of ammonia monohydrate (AMH) solid below 324 K and congruent melting at higher temperatures. The congruent melting is associated with the stability of a previously unobserved solid phase of AMH, which we named AMH-VII. Another, presumably water-rich, hydrate has also been detected in the range 4 GPa–7 GPa at 295 K on decompression of the high pressure disordered ionico-molecular alloy (DIMA) phase. Comparing our melting data to the literature suggests that non-congruent melting extends from 220 K to 324 K and that the solid phase that borders the fluid between 220 K and 270 K, called AMH-III, is not a proper phase of AMH but a solid solution of ammonia hemihydrate and ice. These results allow us to propose a revised and extended experimental phase diagram of AMH." @default.
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• W3092844982 date "2020-10-15" @default.
• W3092844982 modified "2023-10-09" @default.
• W3092844982 title "Melting curve and phase diagram of ammonia monohydrate at high pressure and temperature" @default.
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• W3092844982 doi "https://doi.org/10.1063/5.0021207" @default.
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• W3092844982 hasPublicationYear "2020" @default.
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