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- W3093973781 abstract "Abstract Since the 1970s, high-resolution transmission electron microscopy (HRTEM) is well established as the most appropriate method to explore the structural complexity of niobium tungsten oxides. Today, scanning transmission electron microscopy (STEM) represents an important alternative for performing the structural characterization of such oxides. STEM images recorded with a high-angle annular dark field (HAADF) detector provide not only information about the cation positions but also about the distribution of niobium and tungsten as the intensity is directly correlated to the local scattering potential. The applicability of this method is demonstrated here for the characterization of the real structure of Nb 7 W 10 O 47.5 . This sample contains well-ordered domains of Nb 8 W 9 O 47 and Nb 4 W 7 O 31 besides little ordered areas according to HRTEM results. Structural models for Nb 4 W 7 O 31 and twinning occurring in this phase have been derived from the interpretation of HAADF-STEM images. A remarkable grain boundary between well-ordered domains of Nb 4 W 7 O 31 and Nb 8 W 9 O 47 has been found that contains one-dimensionally periodic features. Furthermore, short-range order observed in less ordered areas could be attributed to an intimate intergrowth of small sections of different tetragonal tungsten bronze (TTB) based structures." @default.
- W3093973781 created "2020-10-29" @default.
- W3093973781 creator A5013336575 @default.
- W3093973781 date "2020-10-15" @default.
- W3093973781 modified "2023-09-23" @default.
- W3093973781 title "Intergrowth of niobium tungsten oxides of the tetragonal tungsten bronze type" @default.
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- W3093973781 doi "https://doi.org/10.1515/znb-2020-0107" @default.
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