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• W3097156904 abstract "Abstract Schiff-base ligand, 2,6-bis(benzimino)-4-phenyl-1,3,5-triazine (L), and its transition metal complexes of Co( ii ), Ni( ii ), and Cu( ii ) were synthesized by refluxing the reaction mixture and its analytical, spectral, and thermogravimetric characteristics were explored by various techniques: AAS, FT-IR, UV-vis, TG-DTG, CHNS/O, and VSM. It was observed that all the metal containing complexes are non-electrolytic, mononuclear, and paramagnetic in nature, confirmed by the molar conductance and magnetic susceptibility measurements. Optical spectral data were used to investigate the geometrical and spectral parameters of [Co(L)(ac) 2 ], [Ni(L)(ac) 2 ], [Cu(L)(ac) 2 ], [Cu(L)(acac) 2 ], and [Cu(L)(fmc) 2 ] complexes. Simultaneous thermal analyses (TG-DTG) in nitrogen atmosphere reveal that the ligand decomposes in one step, [Co(L)(ac) 2 ], [Ni(L)(ac) 2 ], and [Cu(L) (ac) 2 ] complexes are decomposed in three steps, whereas [Cu(L)(acac) 2 ] and [Cu(L) (fmc) 2 ] are decomposed in five and two steps, respectively. In addition, activation energy ( E a ) and pre-exponential factor (ln A ) were evaluated by TG-DTG decomposition steps of compounds using the Coats–Redfern formula. Enthalpy (∆ H ), entropy (∆ S ), and Gibbs free energy (∆ G ) of the as-prepared metal complexes were also speculated by various thermodynamic equations." @default.
• W3097156904 created "2020-11-09" @default.
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• W3097156904 date "2020-10-20" @default.
• W3097156904 modified "2023-10-17" @default.
• W3097156904 title "Synthesis, spectral and thermo-kinetics explorations of Schiff-base derived metal complexes" @default.
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• W3097156904 doi "https://doi.org/10.1515/chem-2020-0168" @default.
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