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• W3100164557 abstract "The previously unknown crystal structure of pingguite was determined and refined from laboratory X-ray powder diffraction data using a synthetic sample. Additional single crystal diffraction of natural pingguite confirms that the crystal structure of the synthetic sample is identical to the natural mineral. This new crystal structure calls for a revised chemistry of the rare mineral pingguite to Bi $$_6$$ Te $$_2$$ O $$_{15}$$ instead of the previously reported formula Bi $$_6$$ Te $$_2$$ O $$_{13}$$ . Pingguite contains Te $$^mathrm{VI}$$ only and not Te $$^mathrm{IV}$$ as previously reported. Pingguite undergoes an irreversible phase transition around 840 $$^{circ }$$ C which is characterized by a loss of oxygen and a reduction from Te $$^mathrm{VI}$$ to Te $$^mathrm{IV}$$ resulting in a $$delta $$ -Bi $$_2$$ O $$_3$$ like type structure. In addition, we report the Raman spectroscopic data on the natural pingguite." @default.
• W3100164557 created "2020-11-23" @default.
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• W3100164557 date "2020-11-19" @default.
• W3100164557 modified "2023-10-16" @default.
• W3100164557 title "Crystal structure and thermal behavior of Bi$$_6$$Te$$_2$$O$$_{15}$$: investigation of synthetic and natural pingguite" @default.
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• W3100164557 doi "https://doi.org/10.1007/s00269-020-01121-7" @default.
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