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- W3100548729 abstract "A novel polyoxomolybdate with a diprotonated porphyrin as counter-cation, namely, 5,10,15,20-tetrakis(4-carboxyphenyl)-21 H ,22 H ,23 H ,24 H -porphine(2+) hexamolybdate(VI) pentahydrate, (C 48 H 32 N 4 O 8 )[Mo 6 O 19 ]·5H 2 O or (H 2 TCPP)[Mo 6 O 19 ]·5H 2 O, I , was prepared via the hydrothermal reaction of MoCl 5 , 5,10,15,20-tetrakis(4-carboxyphenyl)-21 H ,23 H -porphine (TCPP) and distilled water. The crystal structure of hydrated polyoxometalate (POM) salt I was characterized by single-crystal X-ray diffraction. The compound is characterized by an isolated (zero-dimensional, 0D) structure, because it cannot extend via covalent bonds. The structure contains one [Mo 6 O 19 ] 2− anion, one (H 2 TCPP) 2+ cation and five lattice water molecules. Each of the Mo 6+ ions is six-coordinated and displays a distorted octahedral motif. The (H 2 TCPP) 2+ cation displays a distorted saddle motif. A three-dimensional (3D) supramolecular framework is formed via hydrogen-bonding interactions. The compound shows a red photoluminescence emission." @default.
- W3100548729 created "2020-11-23" @default.
- W3100548729 creator A5084049028 @default.
- W3100548729 date "2020-11-09" @default.
- W3100548729 modified "2023-10-13" @default.
- W3100548729 title "Crystal structure and photophysical properties of a novel polyoxomolybdate porphyrin" @default.
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- W3100548729 doi "https://doi.org/10.1107/s2053229620014461" @default.
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