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• W3100893280 endingPage "110754" @default.
• W3100893280 startingPage "110754" @default.
• W3100893280 abstract "High crystalline and well dispersed nano-ZSM-5 was rapidly synthesized in template-free system using high-low temperature two-stage process with as-synthesized silicalite-1 as the seed, and characterized via XRD, SEM, N2 adsorption, FT-IR, Py-IR, TG and so on. Firstly, seed-assisted one-stage crystallization was examined and the results showed that high crystalline nano-ZSM-5 (>90%) could be obtained at 180 °C and 220 °C when the duration time was more than 12 h and 2 h, respectively, but the products tended to be agglomerated with the increase of crystallinity. Based on this, two-stage crystallization was comparatively studied between 220 °C/1 h-180 °C/1–6 h and 220 °C/4 h-180 °C/1–4 h, and high crystalline ZSM-5 (Z-1-6) (97%) with the size of 70–90 nm and good dispersion was synthesized at 220 °C/1 h-180 °C/6 h, while submicron aggregates consisted of 60–120 nm irregular cuboids with high crystallinity (>90%) were obtained at 220 °C/4 h-180 °C/1–4 h. Structural and acidic characterization indicated that Z-1-6 had excellent surface adsorption properties and moderate acidity compared with the commercial micron-ZSM-5. Finally, seed-assisted two-stage crystallization mechanism was proposed about accelerating the depolymerization of silicalite-1 into more smaller nucleation sites and avoiding the aggregation of crystal nuclei by controlling a shorter duration time at a higher temperature and ensuring the stable growth of nano-crystals at a lower temperature." @default.
• W3100893280 created "2020-11-23" @default.
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• W3100893280 date "2021-01-01" @default.
• W3100893280 modified "2023-10-11" @default.
• W3100893280 title "Seed-assisted template-free synthesis of nano-sized ZSM-5 via two-stage crystallization with related investigation of mechanism" @default.
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• W3100893280 doi "https://doi.org/10.1016/j.micromeso.2020.110754" @default.
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